Search results for "Analytical strategy"
showing 4 items of 4 documents
Studying radical organizational innovation through grounded theory
2000
The main aim of this article is to study the social processes occurring during the implementation of radical organizational innovation. Our aim is to understand the nature of the development of radical innovation by identifying the social processes, that are taking place. The perspective for the analysis stems from grounded theory as a generative and inductive analytical strategy (Glaser & Strauss, 1967). An in-depth case study was thoroughly analysed. A total of 14 indepth interviews were conducted with key informants selected according to theoretical sampling criteria. The systematic use of the constant comparative method allowed us to differentiate grounded theories leading to a c…
Identifying Genetic Traces of Historical Expansions: Phoenician Footprints in the Mediterranean
2008
10 páginas, 1 figura, 4 páginas.-- et al.
Determination of the Herbicide Fluometuron by Photo‐induced Chemiluminescence in a Continuous‐flow Multicommutation Assembly
2007
Abstract This study was dealing with the chemiluminometric determination of the selective herbicide Fluometuron or 1,1‐dimethyl‐3‐(α,α,α‐trifluoro‐m‐tolyl)urea, (C10H11F3N2O) with a molecular weight 232.29 belongs to the phenyl urea herbicides family. The analytical strategy is based on the continuous‐flow manifold, multicommutation and the analyte pre‐treatment, the photo‐degradation. The optimization of chemical (pH, medium, temperature, and organized media) and hydrodynamic parameters (volume of reagents and flow rate) was performed by univariant and multiparametric simplex procedure respectively. Analytical figures of merit and the effect of foreign substances were studied. The method r…
Target analysis of primary aromatic amines combined with a comprehensive screening of migrating substances in kitchen utensils by liquid chromatograp…
2015
An analytical strategy including both the quantitative target analysis of 8 regulated primary aromatic amines (PAAs), as well as a comprehensive post-run target screening of 77 migrating substances, was developed for nylon utensils, using liquid chromatography-orbitrap-high resolution mass spectrometry (LC-HRMS) operating in full scan mode. The accurate mass data were acquired with a resolving power of 50,000 FWHM (scan speed, 2 Hz), and by alternating two acquisition events, ESI+ with and without fragmentation. The target method was validated after statistical optimization of the main ionization and fragmentation parameters. The quantitative method presented appropriate performance to be u…